This review highlights developments in the determination of mycotoxins over a period between mid-2013 and mid-2014. It continues in the format of the previous articles of this series, emphasising on analytical methods to determine aflatoxins,Alternaria toxins, ergot alkaloids, fumonisins, ochratoxins, patulin, trichothecenes and zearalenone. The importance of proper sampling and sample preparation is briefly addressed in a dedicated section, while another chapter summarises new methods used to analyse botanicals and spices. As LC-MS/MS instruments are becoming more and more widespread in the determination of multiple classes of mycotoxins, another section is focusing on such newly developed multi-mycotoxin methods. While the wealth of published methods during the 12 month time span makes it impossible to cover every single one, this exhaustive review nevertheless aims to address and briefly discuss the most important developments and trends.
Abhijith, K.S., Ragavanab, K.V. and Thakur, M.S., 2013. Gold nanoparticles enhanced chemiluminescence – a novel approach for sensitive determination of aflatoxin B1. Analytical Methods 5: 4838-4845.
'Gold nanoparticles enhanced chemiluminescence – a novel approach for sensitive determination of aflatoxin B1 ' () 5 Analytical Methods : 4838 -4845.
Abia, W.A., Warth, B., Sulyok, M., Krska, R., Tchana, A., Njobeh, P.B., Turner, P.C., Kouanfack, C., Eyongetah, M., Dutton, M. and Moundipa, P.F., 2013. Bio-monitoring of mycotoxin exposure in Cameroon using a urinary multi-biomarker approach. Food and Chemical Toxicology 62: 927-934.
'Bio-monitoring of mycotoxin exposure in Cameroon using a urinary multi-biomarker approach ' () 62 Food and Chemical Toxicology : 927 -934.
Abu-Bakar, N.B., Makahleh, A. and Saad, B., 2014. Vortex-assisted liquid-liquid microextraction coupled with high performance liquid chromatography for the determination of furfurals and patulin in fruit juices. Talanta 120: 47-54.
'Vortex-assisted liquid-liquid microextraction coupled with high performance liquid chromatography for the determination of furfurals and patulin in fruit juices ' () 120 Talanta : 47 -54.
Amelin, V.G., Karaseva, N.M. and Tret'yakov, A.V., 2013. Chromatographic methods for the determination of mycotoxins in food products. Journal of Analytical Chemistry 68: 195-205.
'Chromatographic methods for the determination of mycotoxins in food products ' () 68 Journal of Analytical Chemistry : 195 -205.
Anfossi, L., Baggiani, C., Giovannoli, C., Biagioli, F., D’Arco, G. and Giraudi G., 2013a. Optimization of a lateral flow immunoassay for the ultrasensitive detection of aflatoxin M1 in milk. Analytica Chimica Acta 772: 75-80.
'Optimization of a lateral flow immunoassay for the ultrasensitive detection of aflatoxin M1 in milk ' () 772 Analytica Chimica Acta : 75 -80.
Anfossi, L., Baggiani, C., Giovannoli, C., D’Arco G. and Giraudi, G., 2013b. Lateral-flow immunoassays for mycotoxins and phycotoxins: a review. Analytical and Bioanalytical Chemistry 405: 467-480.
'Lateral-flow immunoassays for mycotoxins and phycotoxins: a review ' () 405 Analytical and Bioanalytical Chemistry : 467 -480.
Anfossi, L., Di Nardo, F., Giovannoli, C., Passini, C. and Baggiani, C., 2013c. Increased sensitivity of lateral flow immunoassay for ochratoxin A through silver enhancement. Analytical and Bioanalytical Chemistry 405: 9859-9867.
'Increased sensitivity of lateral flow immunoassay for ochratoxin A through silver enhancement ' () 405 Analytical and Bioanalytical Chemistry : 9859 -9867.
Arroyo-Manzanares, N., Huertas-Pérez, J.F., Gámiz-Gracia, L. and García-Campaña, A.M., 2013. A new approach in sample treatment combined with UHPLC-MS/MS for the determination of multiclass mycotoxins in edible nuts and seeds. Talanta 115: 61-67.
'A new approach in sample treatment combined with UHPLC-MS/MS for the determination of multiclass mycotoxins in edible nuts and seeds ' () 115 Talanta : 61 -67.
Arroyo-Manzanares, N., Huertas-Pérez, J.F., García-Campaña, A.M. and Gámiz-Gracia, L., 2014a. Simple methodology for the determination of mycotoxins in pseudocereals, spelt and rice. Food Control 36: 94-101.
'Simple methodology for the determination of mycotoxins in pseudocereals, spelt and rice ' () 36 Food Control : 94 -101.
Arroyo-Manzanares, N., Malysheva, S.V., Vanden Bussche, J., Vanhaecke, L., Di Mavungu, J.D. and De Saeger, S., 2014b. Holistic approach based on high resolution and multiple stage mass spectrometry to investigate ergot alkaloids in cereals. Talanta 118: 359-367.
'Holistic approach based on high resolution and multiple stage mass spectrometry to investigate ergot alkaloids in cereals ' () 118 Talanta : 359 -367.
Asam, S. and Rychlik M., 2013. Potential health hazards due to the occurrence of the mycotoxin tenuazonic acid in infant food. European Food Research and Technology 236: 491-497.
'Potential health hazards due to the occurrence of the mycotoxin tenuazonic acid in infant food ' () 236 European Food Research and Technology : 491 -497.
Asam, S., Habler, K. and Rychlik M., 2013. Determination of tenuazonic acid in human urine by means of a stable isotope dilution assay. Analytical and Bioanalytical Chemistry 405: 4149-4158.
'Determination of tenuazonic acid in human urine by means of a stable isotope dilution assay ' () 405 Analytical and Bioanalytical Chemistry : 4149 -4158.
Ates, E., Godula, M., Stroka, J. and Senyuva, H., 2014. Screening of plant and fungal metabolites in wheat, maize and animal feed using automated on-line clean-up coupled to high resolution mass spectrometry. Food Chemistry 142: 276-284.
'Screening of plant and fungal metabolites in wheat, maize and animal feed using automated on-line clean-up coupled to high resolution mass spectrometry ' () 142 Food Chemistry : 276 -284.
Azaiez, I., Giusti, F., Sagratini, G., Mañes, J. and Fernández-Franzón, M., 2014. Multi-mycotoxins analysis in dried fruit by LC/MS/MS and a modified QuEChERS procedure. Food Analytical Methods 7: 935-945.
'Multi-mycotoxins analysis in dried fruit by LC/MS/MS and a modified QuEChERS procedure ' () 7 Food Analytical Methods : 935 -945.
Bartók, T., Szécsi, A., Juhász, K., Bartók, M. and Mesterházy, A., 2013a. ESI-MS and MS/MS identification of the first ceramide analogues of fumonisin B1 mycotoxin from aFusarium verticillioides culture following RP-HPLC separation. Food Additives and Contaminants Part A 30: 1651-1659.
'ESI-MS and MS/MS identification of the first ceramide analogues of fumonisin B1 mycotoxin from a Fusarium verticillioides culture following RP-HPLC separation ' () 30 Food Additives and Contaminants Part A : 1651 -1659.
Bartók, T., Tölgyesi, L., Szécsi, A., Mesterházy, A., Bartók, M., Gyimes, E. and Véha, A., 2014. Detection of previously unknown fumonisin P analogue mycotoxins in aFusarium verticillioides culture by high-performance liquid chromatography-electrospray ionization time-of-flight and ion trap mass spectrometry. Journal of Chromatographic Science 52: 508-513.
'Detection of previously unknown fumonisin P analogue mycotoxins in a Fusarium verticillioides culture by high-performance liquid chromatography-electrospray ionization time-of-flight and ion trap mass spectrometry ' () 52 Journal of Chromatographic Science : 508 -513.
Bartók, T., Tölgyesi, L., Szécsi, A., Varga, J., Bartók, M., Mesterházy, A., Gyimes, E. and Véha, A., 2013b. Identification of unknown isomers of fumonisin B5 mycotoxin in aFusarium verticillioides culture by high-performance liquid chromatography/electrospray ionization time-of-flight and ion trap mass spectrometry. Journal of Liquid Chromatography and Related Technologies 36: 1549-1561.
'Identification of unknown isomers of fumonisin B5 mycotoxin in a Fusarium verticillioides culture by high-performance liquid chromatography/electrospray ionization time-of-flight and ion trap mass spectrometry ' () 36 Journal of Liquid Chromatography and Related Technologies : 1549 -1561.
Bazin, I., Faucet-Marquis, V., Monje, M.C., El Khoury, M., Marty, J.L. and Pfohl-Leszkowicz, A., 2013. Impact of pH on the stability and the cross-reactivity of ochratoxin A and citrinin. Toxins 5: 2324-2340.
'Impact of pH on the stability and the cross-reactivity of ochratoxin A and citrinin ' () 5 Toxins : 2324 -2340.
Beaulieu, W.T., Panaccione, D.G., Hazekamp, C.S., McKee, M.C., Ryan, K.L. and Clay, K, 2013. Differential allocation of seed-borne ergot alkaloids during early ontogeny of morning glories (Convolvulaceae). Journal of Chemical Ecology 39: 919-930.
'Differential allocation of seed-borne ergot alkaloids during early ontogeny of morning glories (Convolvulaceae) ' () 39 Journal of Chemical Ecology : 919 -930.
Belhassen, H., Jimenez-Diaz, I., Ghali, R., Ghorbel, H., Molina-Molina, J.M., Olea N. and Hedili, A., 2014. Validation of a UHPLC-MS/ MS Method for quantification of zearalenone, alpha-ZEL, beta-ZEL, alpha-ZAL, beta-ZAL and ZAN in human urine. Journal of Chromatography B 962: 68-74.
'Validation of a UHPLC-MS/ MS Method for quantification of zearalenone, alpha-ZEL, beta-ZEL, alpha-ZAL, beta-ZAL and ZAN in human urine ' () 962 Journal of Chromatography B : 68 -74.
Beloglazova N., Shmelin, P., Goryacheva, I. and De Saeger, S., 2013a. Liposomes loaded with quantum dots for ultrasensitive on-site determination of aflatoxin M1 in milk products. Analytical and Bioanalytical Chemistry 405: 7795-7802.
'Liposomes loaded with quantum dots for ultrasensitive on-site determination of aflatoxin M1 in milk products ' () 405 Analytical and Bioanalytical Chemistry : 7795 -7802.
Beloglazova, N.V., Shmelin, P.S., Speranskaya, E.S., Lucas, B., Helmbrecht, C., Knopp, D., Niessner, R., De Saeger, S. and Goryacheva, I.Y., 2013b. Quantum dot loaded liposomes as fluorescent labels for immunoassay. Analytical Chemistry 85: 7197-7204.
'Quantum dot loaded liposomes as fluorescent labels for immunoassay ' () 85 Analytical Chemistry : 7197 -7204.
Beltrán, E., Ibáñez, M., Portolés, T., Ripollés, C., Sancho, J.V., Yusa, V., Marín, S. and Hernández, F., 2013. Development of sensitive and rapid analytical methodology for food analysis of 18 mycotoxins included in a total diet study. Analytica Chimica Acta 783: 39-48.
'Development of sensitive and rapid analytical methodology for food analysis of 18 mycotoxins included in a total diet study ' () 783 Analytica Chimica Acta : 39 -48.
Beltrán, E., Ibáñez, M., Sancho, J.V. and Hernández, F., 2014. Determination of patulin in apple and derived products by UHPLC-MS/MS. Study of matrix effects with atmospheric pressure ionisation sources. Food Chemistry 142: 400-407.
'Determination of patulin in apple and derived products by UHPLC-MS/MS. Study of matrix effects with atmospheric pressure ionisation sources ' () 142 Food Chemistry : 400 -407.
Bergmann, D., Hübner, F. and Humpf, H.U., 2013. Stable isotope dilution analysis of small molecules with carboxylic acid functions using 18O labelling for HPLC-ESI-MS/MS: analysis of fumonisin B1. Journal of Agricultural and Food Chemistry 61: 7904-7908.
'Stable isotope dilution analysis of small molecules with carboxylic acid functions using 18O labelling for HPLC-ESI-MS/MS: analysis of fumonisin B1 ' () 61 Journal of Agricultural and Food Chemistry : 7904 -7908.
Berthiller, F., Burdaspal, P.A., Crews, C., Iha, M.H., Krska, R., Lattanzio, V.M.T., MacDonald, S., Malone, R.J., Maragos, C., Solfrizzo, M., Stroka, J. and Whitaker, T.B., 2014. Developments in mycotoxin analysis: an update for 2012-2013. World Mycotoxin Journal 7: 3-33.
'Developments in mycotoxin analysis: an update for 2012-2013 ' () 7 World Mycotoxin Journal : 3.
Biancardi, A., Piro, R., Dall’Asta, C. and Galaverna, G., 2013. Simple and reliable liquid chromatography-tandem mass spectrometry method for the determination of aflatoxin M1 in milk. Food Additives and Contaminants Part A 30: 381-388.
'Simple and reliable liquid chromatography-tandem mass spectrometry method for the determination of aflatoxin M1 in milk ' () 30 Food Additives and Contaminants Part A : 381 -388.
Breidbach, A., Povilaitye, V., Mischke, C., Doncheva, I., Van Egmond, H. and Stroka, J., 2008. Validation of an analytical method to determine the content of T-2 and HT-2 toxins in cereals and baby food by immunoaffinity column clean-up and GC-MS. JRC Scientific and Technical Reports: EUR 23559 EN-2008.
Brera, C., Pannunzi, E., Guarino, C., Debegnach, F., Gregori, E. and De Santis, B., 2014. Ochratoxin A determination in cured ham by high performance liquid chromatography fluorescence detection and ultra performance liquid chromatography tandem mass spectrometry: a comparative study. Journal of Liquid Chromatography and Related Technologies 37: 2036-2045.
'Ochratoxin A determination in cured ham by high performance liquid chromatography fluorescence detection and ultra performance liquid chromatography tandem mass spectrometry: a comparative study ' () 37 Journal of Liquid Chromatography and Related Technologies : 2036 -2045.
Brezina, U., Valenta, H., Rempe, I., Kersten, S., Humpf, H.U. and Dänicke, S., 2014. Development of a liquid chromatography tandem mass spectrometry method for the simultaneous determination of zearalenone, deoxynivalenol and their metabolites in pig serum. Mycotoxin Research 30: 171-86.
'Development of a liquid chromatography tandem mass spectrometry method for the simultaneous determination of zearalenone, deoxynivalenol and their metabolites in pig serum ' () 30 Mycotoxin Research : 171 -86.
Bryła, M., Jedrzejczak, R., Szymczyk, K., Roszko, M. and Obiedzinski, M. W., 2014. An LC-IT-MS/MS-based method to determine trichothecenes in grain products. Food Analytical Methods 7: 1056-1065.
'An LC-IT-MS/MS-based method to determine trichothecenes in grain products ' () 7 Food Analytical Methods : 1056 -1065.
Bryła, M., Roszko, M., Szymczyk, K., Jedrzejczak, R., Obiedzi?ski, M.W. and Sekul, J., 2013. Fumonisins in plant-origin food and fodder – a review. Food Additives and Contaminants Part A 30: 1626-1640.
'a review ' () 30 Food Additives and Contaminants Part A : 1626 -1640.
Busman, M., Liu, J., Zhong, H., Bobell, J.R. and Maragos, C.M., 2014. Determination of the aflatoxin AFB1 from corn by direct analysis in real time-mass spectrometry (DART-MS). Food Additives and Contaminants Part A 31: 932-939.
'Determination of the aflatoxin AFB1 from corn by direct analysis in real time-mass spectrometry (DART-MS) ' () 31 Food Additives and Contaminants Part A : 932 -939.
Campone, L., Piccinelli, A.L., Celano, R., Russo M. and Rastrelli, L., 2013. Rapid analysis of aflatoxin M1 in milk using dispersive liquid-liquid microextraction coupled with ultrahigh pressure liquid chromatography tandem mass spectrometry. Analytical and Bioanalytical Chemistry 405: 8645-8652.
'Rapid analysis of aflatoxin M1 in milk using dispersive liquid-liquid microextraction coupled with ultrahigh pressure liquid chromatography tandem mass spectrometry ' () 405 Analytical and Bioanalytical Chemistry : 8645 -8652.
Cao, X., Wu, S., Yue, Y., Wang S., Wang, Y., Tao, L., Tian, H., Xie, J. and Ding, H., 2013. A high-throughput method for the simultaneous determination of multiple mycotoxins in human and laboratory animal biological fluids and tissues by PLE and HPLC-MS/MS. Journal of Chromatography B 942-943: 113-125.
'A high-throughput method for the simultaneous determination of multiple mycotoxins in human and laboratory animal biological fluids and tissues by PLE and HPLC-MS/MS ' () 942-943 Journal of Chromatography B : 113 -125.
Capriotti, A.L., Cavaliere, C., Foglia, P., Samperi, R., Stampachiacchiere, S., Ventura, S. and Laganà, A., 2014. Multiclass analysis of mycotoxins in biscuits by high performance liquid chromatography-tandem mass spectrometry. Comparison of different extraction procedures. Journal of Chromatography A 1343: 69-78.
'Multiclass analysis of mycotoxins in biscuits by high performance liquid chromatography-tandem mass spectrometry. Comparison of different extraction procedures ' () 1343 Journal of Chromatography A : 69 -78.
Cheli, F., Battaglia, D., Gallo, R. and Dell’Orto, V., 2014a. EU legislation on cereal safety: an update with a focus on mycotoxins. Food Control 37: 315-325.
'EU legislation on cereal safety: an update with a focus on mycotoxins ' () 37 Food Control : 315 -325.
Cheli, F., Fusi, E. and Baldi, A. 2014b. Cell-based models for mycotoxin screening and toxicity evaluation: an update. World Mycotoxin Journal 7: 153-166.
'Cell-based models for mycotoxin screening and toxicity evaluation: an update ' () 7 World Mycotoxin Journal : 153 -166.
Cheli, F., Pinotti, L., Rossi, L. and Dell’Orto, V., 2013. Effect of milling procedures on mycotoxin distribution in wheat fractions: a review. LWT – Food Science and Technology 54: 307-314.
'Effect of milling procedures on mycotoxin distribution in wheat fractions: a review ' () 54 LWT – Food Science and Technology : 307 -314.
Chen, X., Huang, Y., Duan, N., Wu, S., Xia, Y., Ma, X., Zhu, C., Jiang, Y., Ding, Z. and Wang, Z., 2014. Selection and characterization of single stranded DNA aptamers recognizing fumonisin B1. Microchimica Acta 181: 1317-1324.
'Selection and characterization of single stranded DNA aptamers recognizing fumonisin B1 ' () 181 Microchimica Acta : 1317 -1324.
De Angelis, E., Monaci, L. and Visconti, A., 2014a. Investigation on the stability of deoxynivalenol and DON-3 glucoside during gastro-duodenalin vitro digestion of a naturally contaminated bread model food. Food Control 43: 270-275.
'Investigation on the stability of deoxynivalenol and DON-3 glucoside during gastro-duodenal in vitro digestion of a naturally contaminated bread model food ' () 43 Food Control : 270 -275.
De Angelis, E., Monaci, L., Mackie, A., Salt, L. and Visconti, A., 2014b. Bioaccessibility of T-2 and HT-2 toxins in mycotoxin contaminated bread models submitted toin vitro human digestion. Innovative Food Science and Emerging Technologies 22: 248-256.
'Bioaccessibility of T-2 and HT-2 toxins in mycotoxin contaminated bread models submitted to in vitro human digestion ' () 22 Innovative Food Science and Emerging Technologies : 248 -256.
De Angelis, E., Monaci, L., Pascale, M. and Visconti, A., 2013. Fate of deoxynivalenol, T-2 and HT-2 toxins and their glucoside conjugates from flour to bread: an investigation by high-performance liquid chromatography high-resolution mass spectrometry. Food Additives and Contaminants Part A 30: 345-355.
'Fate of deoxynivalenol, T-2 and HT-2 toxins and their glucoside conjugates from flour to bread: an investigation by high-performance liquid chromatography high-resolution mass spectrometry ' () 30 Food Additives and Contaminants Part A : 345 -355.
De Girolamo, A., Lattanzio, V.M.T., Schena, R., Visconti, A. and Pascale, M., 2014. Use of liquid chromatography-high-resolution mass spectrometry for isolation and characterization of hydrolyzed fumonisins and relevant analysis in maize-based products Journal of Mass Spectrometry 49: 297-305.
'Use of liquid chromatography-high-resolution mass spectrometry for isolation and characterization of hydrolyzed fumonisins and relevant analysis in maize-based products ' () 49 Journal of Mass Spectrometry : 297 -305.
De Girolamo, A., Solfrizzo, M., Lattanzio, V.M.T., Stroka, J., Alldrick, A., Van Egmond, H.P. and Visconti, A., 2013. Critical evaluation of LC-MS-based methods for simultaneous determination of deoxynivalenol, ochratoxin A, zearalenone, aflatoxins, fumonisins and T-2/HT-2 toxins in maize. World Mycotoxin Journal 6: 317-334.
'Critical evaluation of LC-MS-based methods for simultaneous determination of deoxynivalenol, ochratoxin A, zearalenone, aflatoxins, fumonisins and T-2/HT-2 toxins in maize ' () 6 World Mycotoxin Journal : 317 -334.
De Oliveira, D.N., Ferreira, M.S. and Catharino, R.R., 2014. Rapid and simultaneousin situ assessment of aflatoxins and stilbenes using silica plate imprinting mass spectrometry imaging. PLoS ONE 9: e90901.
'Rapid and simultaneous in situ assessment of aflatoxins and stilbenes using silica plate imprinting mass spectrometry imaging ' () 9 PLoS ONE : e90901.
Della Riccia, G. and Del Zotto, S., 2013. A multivariate regression model for detection of fumonisins content in maize from near infrared spectra. Food Chemistry 141: 4289-4294.
'A multivariate regression model for detection of fumonisins content in maize from near infrared spectra ' () 141 Food Chemistry : 4289 -4294.
Desmarchelier, A., Tessiot, S., Bessaire, T., Racault, L., Fiorese, E., Urbani, A., Chan, W.C., Cheng, P. and Mottier, P., 2014. Combining the quick, easy, cheap, effective, rugged and safe approach and clean-up by immunoaffinity column for the analysis of 15 mycotoxins by isotope dilution liquid chromatography tandem mass spectrometry. Journal of Chromatography A 1337: 75-84.
'Combining the quick, easy, cheap, effective, rugged and safe approach and clean-up by immunoaffinity column for the analysis of 15 mycotoxins by isotope dilution liquid chromatography tandem mass spectrometry ' () 1337 Journal of Chromatography A : 75 -84.
Di Mavungu, J.D., Malysheva, S.V., Sanders, M., Larionova, D., Robbens, J., Dubruel, P., Van Peteghem, C. and De Saeger, S., 2012. Development and validation of a new LC-MS/MS method for the simultaneous determination of six major ergot alkaloids and their corresponding epimers. Application to some food and feed commodities. Food Chemistry 135: 292-303.
'Development and validation of a new LC-MS/MS method for the simultaneous determination of six major ergot alkaloids and their corresponding epimers. Application to some food and feed commodities ' () 135 Food Chemistry : 292 -303.
Dohnal, V., Dvořák, V., Malíř, F., Ostrý, V. and Roubal T., 2013. A comparison of ELISA and HPLC methods for determination of ochratoxin A in human blood serum in the Czech Republic. Food Chemical Toxicology 62: 427-431.
'A comparison of ELISA and HPLC methods for determination of ochratoxin A in human blood serum in the Czech Republic ' () 62 Food Chemical Toxicology : 427 -431.
D’Orazio, G., Asensio-Ramos, M., Hernandez-Borges, J., Fanali, S. and Rodriguez-Delgado, M.A., 2014. Estrogenic compounds determination in water samples by dispersive liquid-liquid microextraction and micellar electrokinetic chromatography coupled to mass spectrometry. Journal of Chromatography A 1344: 109-121.
'Estrogenic compounds determination in water samples by dispersive liquid-liquid microextraction and micellar electrokinetic chromatography coupled to mass spectrometry ' () 1344 Journal of Chromatography A : 109 -121.
Drzymala, S., Riedel, J., Köppen, R., Garbe, L.A. and Koch, M., 2014. Preparation of C-13-labelled cis-zearalenone and its application as internal standard in stable isotope dilution analysis. World Mycotoxin Journal 7: 45-52.
'Preparation of C-13-labelled cis-zearalenone and its application as internal standard in stable isotope dilution analysis ' () 7 World Mycotoxin Journal : 45 -52.
Dzantiev, B.B., Byzova, N.A., Urusov, A.E. and Zherdev, A.V., 2014. Immunochromatographic methods in food analysis. Trends in Analytical Chemistry 55: 81-93.
'Immunochromatographic methods in food analysis ' () 55 Trends in Analytical Chemistry : 81 -93.
Dzuman, Z., Vaclavikova, M., Polisenska, I., Veprikova, Z., Fenclova, M., Zachariasova, M. and Hajslova, J., 2014a. Enzyme-linked immunosorbent assay in analysis of deoxynivalenol: investigation of the impact of sample matrix on results accuracy. Analytical and Bioanalytical Chemistry 406: 505-514.
'Enzyme-linked immunosorbent assay in analysis of deoxynivalenol: investigation of the impact of sample matrix on results accuracy ' () 406 Analytical and Bioanalytical Chemistry : 505 -514.
Dzuman, Z., Zachariasova, M., Lacina, O., Veprikova, Z., Slavikova, P. and Hajslova, J., 2014b. A rugged high-throughput analytical approach for the determination and quantification of multiple mycotoxins in complex feed matrices. Talanta 121: 263-272.
'A rugged high-throughput analytical approach for the determination and quantification of multiple mycotoxins in complex feed matrices ' () 121 Talanta : 263 -272.
Edupuganti, S.R., Edupuganti, O.P. and O’Kennedy, R., 2013a. Generation of anti-zearalenone scFv and its incorporation into surface plasmon resonance-based assay for the detection of zearalenone in sorghum. Food Control 34: 668-674.
'Generation of anti-zearalenone scFv and its incorporation into surface plasmon resonance-based assay for the detection of zearalenone in sorghum ' () 34 Food Control : 668 -674.
Edupuganti, S.R., Edupuganti, O.P., Hearty, S. and O’Kennedy, R., 2013b. A highly stable, sensitive, regenerable and rapid immunoassay for detecting aflatoxin B1 in corn in corporating covalent AFB1 immobilization and a recombinant fab antibody. Talanta 115: 329-335.
'A highly stable, sensitive, regenerable and rapid immunoassay for detecting aflatoxin B1 in corn in corporating covalent AFB1 immobilization and a recombinant fab antibody ' () 115 Talanta : 329 -335.
European Committee for Standardization (CEN), 2011. Food analysis – performance criteria for single laboratory validated methods of analysis for the determination of mycotoxins. Technical Report: CEN/TR 16059.
European Food Safety Authority (EFSA) 2012. Panel on Contaminants in the Food Chain, Scientific Opinion on Ergot alkaloids in food and feed. EFSA Journal 10: 2798.
European Food Safety Authority (EFSA) 2013a. Panel on Contaminants in the Food Chain, Scientific opinion on risks for animal and public health related to the presence of nivalenol in food and feed. EFSA Journal 11: 3262.
European Food Safety Authority (EFSA) 2013b. Panel on Contaminants in the Food Chain, Statement on the risks for public health related to a possible increase of the maximum level of deoxynivalenol for certain semi-processed cereal products. EFSA Journal 11: 3490.
Ezekiel, C.N., Warth, B., Ogara, I.M., Abia, W.A., Ezekiel, V.C., Atehnkeng, J., Sulyok, M., Turner, P.C., Tayo, G.O.,Krska, R. and Bandyopadhyay, R., 2014. Mycotoxin exposure in rural residents in Northern Nigeria: a pilot study using multi-urinary biomarkers. Environment International 66: 138-345.
'Mycotoxin exposure in rural residents in Northern Nigeria: a pilot study using multi-urinary biomarkers ' () 66 Environment International : 138 -345.
Falavigna, C., Lazzaro, I., Galaverna, G., Battilani, P. and Dall’Asta, C., 2013. Fatty acid esters of fumonisins: first evidence of their presence in maize. Food Additives and Contaminants Part A 30: 1606-1613.
'Fatty acid esters of fumonisins: first evidence of their presence in maize ' () 30 Food Additives and Contaminants Part A : 1606 -1613.
Fang, L.X., Xiong, A.Z., Wang, R., Ji, S., Yang, L. and Wang, Z.T., 2013. A strategy for screening and identifying mycotoxins in herbal medicine using ultra-performance liquid chromatography with tandem quadrupole time-of-flight mass spectrometry. Journal of Separation Science 36: 3115-3122.
'A strategy for screening and identifying mycotoxins in herbal medicine using ultra-performance liquid chromatography with tandem quadrupole time-of-flight mass spectrometry ' () 36 Journal of Separation Science : 3115 -3122.
Fox, G. and Manley, M., 2014. Applications of single kernel conventional and hyperspectral imaging near infrared spectroscopy in cereals. Journal of the Science of Food and Agriculture 94: 174-179.
'Applications of single kernel conventional and hyperspectral imaging near infrared spectroscopy in cereals ' () 94 Journal of the Science of Food and Agriculture : 174 -179.
Gan, N., Zhou, J., Xiong, P., Hu, F., Cao, Y., Li, T. and Jiang, Q., 2013. An ultrasensitive electrochemiluminescent immunoassay for aflatoxin M1 in milk, based on extraction by magnetic graphene and detection by antibody-labelled CdTe quantum dots-carbon nanotubes nanocomposite. Toxins 5: 865-883.
'An ultrasensitive electrochemiluminescent immunoassay for aflatoxin M1 in milk, based on extraction by magnetic graphene and detection by antibody-labelled CdTe quantum dots-carbon nanotubes nanocomposite ' () 5 Toxins : 865 -883.
Geng, Z., Yang, D., Zhou, M., Zhang, P., Wang, D., Liu, F., Zhu, Y. and Zhang, M., 2014. Determination of deoxynivalenol-3-glucoside in cereals by hydrophilic interaction chromatography with ultraviolet detection. Food Analytical Methods 7: 1139-1146.
'Determination of deoxynivalenol-3-glucoside in cereals by hydrophilic interaction chromatography with ultraviolet detection ' () 7 Food Analytical Methods : 1139 -1146.
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Zhao, X., Yuan, Y., Zhang, X. and Yue, T. 2014a. Identification of ochratoxin A in Chinese spices using HPLC fluorescent detectors with immunoaffinity column cleanup. Food Control 46: 332-337.
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This review highlights developments in the determination of mycotoxins over a period between mid-2013 and mid-2014. It continues in the format of the previous articles of this series, emphasising on analytical methods to determine aflatoxins,Alternaria toxins, ergot alkaloids, fumonisins, ochratoxins, patulin, trichothecenes and zearalenone. The importance of proper sampling and sample preparation is briefly addressed in a dedicated section, while another chapter summarises new methods used to analyse botanicals and spices. As LC-MS/MS instruments are becoming more and more widespread in the determination of multiple classes of mycotoxins, another section is focusing on such newly developed multi-mycotoxin methods. While the wealth of published methods during the 12 month time span makes it impossible to cover every single one, this exhaustive review nevertheless aims to address and briefly discuss the most important developments and trends.
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