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This review summarises developments in the determination of mycotoxins over a period between mid-2015 and mid-2016. Analytical methods to determine aflatoxins,Alternaria toxins, ergot alkaloids, fumonisins, ochratoxins, patulin, trichothecenes and zearalenone are covered in individual sections. Advances in proper sampling strategies are discussed in a dedicated section, as are methods used to analyse botanicals and spices and newly developed liquid chromatography mass spectrometry based multi-mycotoxin methods. This critical review aims to briefly discuss the most important recent developments and trends in mycotoxin determination as well as to address limitations of presented methodologies.
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'Tailoring molecularly imprinted polymer beads for alternariol recognition and analysis by a screening with mycotoxin surrogates ' () 1425 Journal of Chromatography A : 231 -239.
Afzali, D. and Fathirad, F., 2016. Determination of zearalenone with a glassy carbon electrode modified with nanocomposite consisting of palladium nanoparticles and a conductive polymeric ionic liquid. Microchimica Acta 183: 2633-2638.
'Determination of zearalenone with a glassy carbon electrode modified with nanocomposite consisting of palladium nanoparticles and a conductive polymeric ionic liquid ' () 183 Microchimica Acta : 2633 -2638.
Afzali, D., Padash, M. and Mostafavi, A., 2015. Determination of trace amounts of zearalenone in beverage samples with an electrochemical sensor. Mycotoxin Research 31: 203-208.
'Determination of trace amounts of zearalenone in beverage samples with an electrochemical sensor ' () 31 Mycotoxin Research : 203 -208.
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'Occurrence of aflatoxin B1 in conventional and organic flour in Italy and the role of sampling ' () 50 Food Control : 858 -863.
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'Development of a rapid LC-MS/MS method for the determination of emerging fusarium mycotoxins enniatins and beauvericin in human biological fluids ' () 7 Toxins : 3554 -3571.
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Bernhardt, K., Valenta, H., Kersten, S., Humpf, H. and Dänicke, S., 2016. Determination of T-2 toxin, HT-2 toxin, and three other type A trichothecenes in layer feed by high-performance liquid chromatography-tandem mass spectrometry (LC-MS/MS) – comparison of two sample preparation methods. Mycotoxin Research 32: 89-97.
'Determination of T-2 toxin, HT-2 toxin, and three other type A trichothecenes in layer feed by high-performance liquid chromatography-tandem mass spectrometry (LC-MS/MS) – comparison of two sample preparation methods ' () 32 Mycotoxin Research : 89 -97.
Berthiller, F., Brera, C., Crews, C., Iha, M.H., Krska, R., Lattanzio, V.M.T., MacDonald, S., Malone, R.J., Maragos, C., Solfrizzo, M., Stroka, J. and Whitaker, T.B., 2016. Developments in mycotoxin analysis: an update for 2014-2015. World Mycotoxin Journal 9: 5-30.
'Developments in mycotoxin analysis: an update for 2014-2015 ' () 9 World Mycotoxin Journal : 5 -30.
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Bueno, D., Istamboulie, G., Munoz, R. and Marty, J.L., 2015. Determination of mycotoxins in food: a review of bioanalytical to analytical methods. Applied Spectroscopy Reviews 50: 728-774.
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Campone, L., Piccinelli, A.L., Celano, R., Pagano, I., Russo, M. and Rastrelli, L., 2016. Rapid and automated analysis of aflatoxin M1 in milk and dairy products by online solid phase extraction coupled to ultra-high-pressure-liquid-chromatography tandem mass spectrometry. Journal of Chromatography A 1428: 212-219.
'Rapid and automated analysis of aflatoxin M1 in milk and dairy products by online solid phase extraction coupled to ultra-high-pressure-liquid-chromatography tandem mass spectrometry ' () 1428 Journal of Chromatography A : 212 -219.
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'Simultaneous determination of naturally occurring estrogens and mycoestrogens in milk by ultrahigh-performance liquid chromatography-tandem mass spectrometry analysis ' () 63 Journal of Agricultural and Food Chemistry : 8940 -8946.
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Chen, Y., Chen, Q., Han, M., Zhou, J., Gong, L., Niu, Y., Zhang, Y., He, L. and Zhang, L., 2016. Development and optimization of a multiplex lateral flow immunoassay for the simultaneous determination of three mycotoxins in corn, rice and peanut. Food Chemistry 213: 478-484.
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De Clercq, N., Van Pamel, E., Van Coillie, E., Vlaemynck, G., Devlieghere, F., Meulenaer, B. and Daeseleire, E., 2016. Optimization and validation of a method without alkaline clean-up for patulin analysis on apple puree agar medium (APAM) and apple products. Food Analytical Methods 9: 370-377.
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De Dominicis, E., Commissati, I., Gritti, E., Catellani, D. and Suman, M., 2015. Quantitative targeted and retrospective data analysis of relevant pesticides, antibiotics and mycotoxins in bakery products by liquid chromatography-single-stage Orbitrap mass spectrometry. Food Additives and Contaminants Part A 32: 1617-1627.
'Quantitative targeted and retrospective data analysis of relevant pesticides, antibiotics and mycotoxins in bakery products by liquid chromatography-single-stage Orbitrap mass spectrometry ' () 32 Food Additives and Contaminants Part A : 1617 -1627.
D’Orazio, G., Asensio-Ramos, M., Hernandez-Borges, J., Rodriguez-Delgado, M.A. and Fanali, S., 2015. Evaluation of the combination of a dispersive liquid-liquid microextraction method with micellar electrokinetic chromatography coupled to mass spectrometry for the determination of estrogenic compounds in milk and yogurt. Electrophoresis 36: 615-625.
'Evaluation of the combination of a dispersive liquid-liquid microextraction method with micellar electrokinetic chromatography coupled to mass spectrometry for the determination of estrogenic compounds in milk and yogurt ' () 36 Electrophoresis : 615 -625.
Escrivá, L., Manyes, L., Font, G. and Berrada, H., 2016. Analysis of trichothecenes in laboratory rat feed by gas chromatography-tandem mass spectrometry. Food Additives and Contaminants Part A 33: 329-338.
'Analysis of trichothecenes in laboratory rat feed by gas chromatography-tandem mass spectrometry ' () 33 Food Additives and Contaminants Part A : 329 -338.
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'Comparison of approaches to deal with matrix effects in LC-MS/MS based determinations of mycotoxins in food and feed ' () 9 World Mycotoxin Journal : 149 -161.
Fan, C., Cao, X., Liu, M. and Wang, W., 2016. Determination ofAlternaria mycotoxins in wine and juice using ionic liquid modified countercurrent chromatography as a pretreatment method followed by high-performance liquid chromatography. Journal of Chromatography A 1436: 133-140.
'Determination ofAlternaria mycotoxins in wine and juice using ionic liquid modified countercurrent chromatography as a pretreatment method followed by high-performance liquid chromatography ' () 1436 Journal of Chromatography A : 133 -140.
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Fraeyman, S., Devreese, M., Broekaert, N., De Mil, T., Antonissen, G., De Baere, S., De Backer, P., Rychlik, M. and Croubels, S., 2015. Journal of Agricultural and Food Chemistry 63: 8560-8567.
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'Survey ofAlternaria toxin contamination in food from the German market, using a rapid HPLC-MS/MS approach ' () 32 Mycotoxin Research : 7 -18.
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This review summarises developments in the determination of mycotoxins over a period between mid-2015 and mid-2016. Analytical methods to determine aflatoxins,Alternaria toxins, ergot alkaloids, fumonisins, ochratoxins, patulin, trichothecenes and zearalenone are covered in individual sections. Advances in proper sampling strategies are discussed in a dedicated section, as are methods used to analyse botanicals and spices and newly developed liquid chromatography mass spectrometry based multi-mycotoxin methods. This critical review aims to briefly discuss the most important recent developments and trends in mycotoxin determination as well as to address limitations of presented methodologies.
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