Möchten Sie über diese Zeitschrift informiert bleiben? Klicken Sie bitte auf die Buttons, um unsere Alerts zu abonnieren.
Möchten Sie über diese Zeitschrift informiert bleiben? Klicken Sie bitte auf die Buttons, um unsere Alerts zu abonnieren.
Deoxynivalenol and nivalenol analysis in soybean and soy flour
in World Mycotoxin JournalSearch for other papers by G. Barros in
Current site
Google Scholar
Search for other papers by D. García in
Current site
Google Scholar
Search for other papers by S. Oviedo in
Current site
Google Scholar
Search for other papers by M. Ramirez in
Current site
Google Scholar
Search for other papers by A. Torres in
Current site
Google Scholar
Search for other papers by S. Chulze in
Current site
Google Scholar
A rapid and accurate method of quantifying deoxynivalenol (DON) and nivalenol (NIV) in soybean and soy flour is described. The samples were extracted with acetonitrile:water (84:16, v/v) and cleaned through a solidphase extraction (SPE) column. The mycotoxins were separated, detected and quantified by reversed-phase high performance liquid chromatography (HPLC) with UV detection (220 nm) using water:methanol (88:12, v/v) as mobile phase. Characteristics of this in-house method such as accuracy, precision and detection and quantification limits were defined by means of a recovery test with spiked soybean and soy flour samples. The detection limit (LOD) was 0.1 µg/g for DON and 0.2 µg/g for NIV, based on a signal-noise ratio 3:1. Quantification limit (LOQ) was established as three times the detection limit.
Kauf
Sofortzugang erwerben (PDF-Download und unbegrenzter Online-Zugang):
Institutszugang
Melden Sie sich mit Open Athens, Shibboleth oder Ihren institutionellen Anmeldedaten an.
Persönliche Anmeldung
Melden Sie sich mit Ihrem brill.com-Konto an
-
Berger, U., Oehme, M. and Kuhn F., 1999. Quantitative determination and structure elucidation of type A- and type B- trichothecenes by HPLC/ion trap multiple mass spectrometry. Journal of Agricultural and Food Chemistry 47: 4240-4245.
'Quantitative determination and structure elucidation of type A- and type B- trichothecenes by HPLC/ion trap multiple mass spectrometry ' () 47 Journal of Agricultural and Food Chemistry : 4240 -4245 .
-
Cahill, L.M., Kruger, S.C., McAlice, B.T., Ramsey, C.S., Prioli, R. and Kohn B., 1999. Quantification of deoxynivalenol in wheat using an immunoaffinity column and liquid chromatography. Journal of Chromatography A 859: 23-28.
'Quantification of deoxynivalenol in wheat using an immunoaffinity column and liquid chromatography ' () 859 Journal of Chromatography A : 23 -28 .
-
DeNijs, M., Rombouts, F. and Notermans, S., 1996. Fusarium molds and their mycotoxins. Journal of Food Safety 16: 15-58.
'Fusarium molds and their mycotoxins ' () 16 Journal of Food Safety : 15 -58 .
-
Dietrich, R., Schneider, E., Usleber, E. and Martlbauer, E., 1995. Use of monoclonal antibody for the analysis of mycotoxins. Natural Toxins 3: 288-293.
'Use of monoclonal antibody for the analysis of mycotoxins ' () 3 Natural Toxins : 288 -293 .
-
European Commission (EC), 2006. Commission Recommendation 576/2006/EC of 17 August 2006 on the presence of deoxynivalenol, zearalenone, ochratoxin A, T-2 and HT-2 and fumonisins in products intended for animal feeding. Official Journal of the European Union L 229/7.
-
Food and Agriculture Organization of the United Nations (FAO), 2004. Animal production and health: protein sources for the animal feed industry. Available at: ftp://ftp.fao.org/docrep/fao/007/y5019e/ y5019e00.pdf.
-
Glenn, A.E., 2007. Mycotoxigenic Fusarium species in animal feed. Animal Feed Science and Technology 137: 213-240.
'Mycotoxigenic Fusarium species in animal feed ' () 137 Animal Feed Science and Technology : 213 -240 .
-
Hepperly, P.R., 1985. Fusarium species and their association with soybean seed under humid tropical conditions in Puerto Rico. Journal of the Agriculture of the University of Puerto Rico 79: 25-33.
'Fusarium species and their association with soybean seed under humid tropical conditions in Puerto Rico ' () 79 Journal of the Agriculture of the University of Puerto Rico : 25 -33 .
-
Josephs, R.D., Schuhmacher, R. and Krska, R., 2001. International interlaboratory study for determination of Fusarium mycotoxins zearalenone and deoxynivalenol in agricultural commodities. Food Additives and Contaminants 18: 417-430.
'International interlaboratory study for determination of Fusarium mycotoxins zearalenone and deoxynivalenol in agricultural commodities ' () 18 Food Additives and Contaminants : 417 -430 .
-
Lauren, D.R. and Greenhalgh, R., 1987. Simultaneous analysis of nivalenol and deoxynivalenol in cereals by liquid chromatography. Journal of AOAC International 70: 479-483.
'Simultaneous analysis of nivalenol and deoxynivalenol in cereals by liquid chromatography ' () 70 Journal of AOAC International : 479 -483 .
-
Malone, B.R., Humphrey, C.W., Romer, T.R. and Richard, J.L., 1998. One-step solid-phase extraction cleanup and fluorometric analysis of deoxynivalenol in grains. Journal of AOAC International 81: 448-451.
'One-step solid-phase extraction cleanup and fluorometric analysis of deoxynivalenol in grains ' () 81 Journal of AOAC International : 448 -451 .
-
Pitt, J.I. and Hocking, A.D. (eds.), 1999. Fungi and food spoilage. Aspen Publ. Inc., Gaithersburg, Maryland.
Fungi and food spoilage , ().
-
Placinta, C.M., D'Mello, J.P.F. and Macdonald, A.M.C., 1999. A review of worldwide contamination of cereal grains and animal feed with Fusarium mycotoxins. Animal Feed Science and Technology 78: 21-37.
'A review of worldwide contamination of cereal grains and animal feed with Fusarium mycotoxins ' () 78 Animal Feed Science and Technology : 21 -37 .
-
Plattner, R.D., 1999. HPLC/MS analysis of Fusarium mycotoxins, fumonisins and deoxynivalenol. Natural Toxins 7: 365-370.
'HPLC/MS analysis of Fusarium mycotoxins, fumonisins and deoxynivalenol ' () 7 Natural Toxins : 365 -370 .
-
Richardson, K.E., Hagler, W.M., Haney, C.A. and Hamilton, P.B., 1985. Zearalenone and trichothecene production in soybeans by toxigenic Fusarium. Journal of Food Protection 48: 240-243.
'Zearalenone and trichothecene production in soybeans by toxigenic Fusarium ' () 48 Journal of Food Protection : 240 -243 .
-
Rotter, B.A., Prelusky, D.B. and Pestka, J.J., 1996. Toxicology of deoxynivalenol (vomitoxin). Journal of Toxicology Environmental 48: 1-34.
'Toxicology of deoxynivalenol (vomitoxin) ' () 48 Journal of Toxicology Environmental : 1 -34 .
-
Ryu, J.C., Ohtsubo, K., Izumiyama, N., Nakamura, K., Tanaka, T., Yamamura, H. and Ueno, Y., 1988. The acute and chronic toxicities of nivalenol in mice. Fundamentals in Applied Toxicology 11: 38-47.
'The acute and chronic toxicities of nivalenol in mice ' () 11 Fundamentals in Applied Toxicology : 38 -47 .
-
Schollenberger, M., Müller, H.-M., Rüfle, M., Terry-Jara, H., Suchy, S., Plank, S. and Drochner, W., 2007. Natural occurrence of Fusarium toxins in soy food marketed in Germany. International Journal of Food Microbiology 113: 142-146.
'Natural occurrence of Fusarium toxins in soy food marketed in Germany ' () 113 International Journal of Food Microbiology : 142 -146 .
-
Schollenberger, M., Müller, H.-M., Rüfle, M., Suchy, S., Plank, S. and Drochner, W., 2006. Natural occurrence of 16 Fusarium toxins in grains and feedstuffs of plant origin from Germany. Mycopathologia 161: 43-52.
'Natural occurrence of 16 Fusarium toxins in grains and feedstuffs of plant origin from Germany ' () 161 Mycopathologia : 43 -52 .
-
Scott, P.M., Lombaert, G.A., Pellaers, P., Bacler, S., Kanhere, S.R., Sun, W.F., Lau, P.Y. and Weber, D., 1989. Application of capillary gas chromatography to a survey of wheat for five trichothecenes. Food Additives and Contaminants 6: 489-500.
'Application of capillary gas chromatography to a survey of wheat for five trichothecenes ' () 6 Food Additives and Contaminants : 489 -500 .
-
Scott, P.M., Lau, P.Y. and Kanhere, S.R., 1981. Gas chromatography with electron capture and mass spectrometric detection of deoxynivalenol in wheat and other grains. Journal of AOAC International 64: 1364-1371.
'Gas chromatography with electron capture and mass spectrometric detection of deoxynivalenol in wheat and other grains ' () 64 Journal of AOAC International : 1364 -1371 .
-
Secretaría de Agricultura Ganadería Pesca y Alimentación de la Nación (SAGPyA), 2007. Soja Informe general. Available at: http:// www.sagyp. mecon.gov.ar/new/0-0/agricultura/otros/estimaciones/ soja/infsoja/php. Accessed 27 April 2007. http://www.sagyp.mecon.gov.ar/new/0-0/agricultura/otros/estimaciones/soja/infsoja/php
-
Shirai, Y., Ono, Y. and Akimoto, K., 2000. Simultaneous determination of deoxynivalenol and nivalenol in grain by high performance liquid chromatography with multifunctional clean-up column for purification. Research Report Animal Feed 26: 1-9.
'Simultaneous determination of deoxynivalenol and nivalenol in grain by high performance liquid chromatography with multifunctional clean-up column for purification ' () 26 Research Report Animal Feed : 1 -9 .
-
Sugita-Konsihi, Y., Tanaka, T., Tabata, S., Nakajima, M., Nouno, M., Nakaie, Y., Chonan, T., Aoyagi, M., Kibune, N., Mizuno, K., Ishikuro, E., Kanamaru, N., Minamisawa, M., Aita, N., Kushiro, M., Tanaka, K. and Takatori, K., 2006. Validation of an HPLC analytical method coupled to a functional clean-up column for determination of deoxynivalenol. Mycopathologia 161: 239-243.
'Validation of an HPLC analytical method coupled to a functional clean-up column for determination of deoxynivalenol ' () 161 Mycopathologia : 239 -243 .
-
Tanaka, T., Yoneda, A., Inoue, S., Sugiura, Y. and Ueno, Y., 2000. Simultaneous determination of thichothecene mycotoxins and zearalenone in cereals by gas chromatography-mass spectrometry. Journal of Chromatography A 882: 23-28.
'Simultaneous determination of thichothecene mycotoxins and zearalenone in cereals by gas chromatography-mass spectrometry ' () 882 Journal of Chromatography A : 23 -28 .
-
Trucksess, M.W., Page, S.W., Wood, G.E. and Cho, T.H., 1998. Determination of deoxynivalenol in whiter flour, whole wheat flour and bran by solid-phase extraction/liquid chromatography: Interlaboratory study. Journal of AOAC International 81: 880-886.
'Determination of deoxynivalenol in whiter flour, whole wheat flour and bran by solid-phase extraction/liquid chromatography: Interlaboratory study ' () 81 Journal of AOAC International : 880 -886 .
| Insgesamt | Letzte 365 Tage | In den letzten 30 Tagen | |
|---|---|---|---|
| Aufrufe von Kurzbeschreibungen | 215 | 105 | 19 |
| Gesamttextansichten | 22 | 1 | 0 |
| PDF-Downloads | 16 | 0 | 0 |
Deoxynivalenol and nivalenol analysis in soybean and soy flour
in World Mycotoxin JournalSearch for other papers by G. Barros in
Current site
Google Scholar
PubMed
Search for other papers by D. García in
Current site
Google Scholar
PubMed
Search for other papers by S. Oviedo in
Current site
Google Scholar
PubMed
Search for other papers by M. Ramirez in
Current site
Google Scholar
PubMed
Search for other papers by A. Torres in
Current site
Google Scholar
PubMed
Search for other papers by S. Chulze in
Current site
Google Scholar
PubMed
A rapid and accurate method of quantifying deoxynivalenol (DON) and nivalenol (NIV) in soybean and soy flour is described. The samples were extracted with acetonitrile:water (84:16, v/v) and cleaned through a solidphase extraction (SPE) column. The mycotoxins were separated, detected and quantified by reversed-phase high performance liquid chromatography (HPLC) with UV detection (220 nm) using water:methanol (88:12, v/v) as mobile phase. Characteristics of this in-house method such as accuracy, precision and detection and quantification limits were defined by means of a recovery test with spiked soybean and soy flour samples. The detection limit (LOD) was 0.1 µg/g for DON and 0.2 µg/g for NIV, based on a signal-noise ratio 3:1. Quantification limit (LOQ) was established as three times the detection limit.
| Insgesamt | Letzte 365 Tage | In den letzten 30 Tagen | |
|---|---|---|---|
| Aufrufe von Kurzbeschreibungen | 215 | 105 | 19 |
| Gesamttextansichten | 22 | 1 | 0 |
| PDF-Downloads | 16 | 0 | 0 |
